|
Uncertainties
for:
Uncertainty
Budget for SPRT's
| 2/3/2000 |
Ar |
Hg |
Ga |
In |
Sn |
Cd |
Zn |
Al |
Ag |
Type
A (in mK)
|
|
|
|
|
|
|
|
|
|
| Bridge
Measurement |
|
|
|
|
|
|
|
|
|
| DR
from DT |
0 |
0 |
0 |
0 |
0 |
0 |
0 |
0 |
0.01 |
| realization
of repeatability |
0.03 |
0.07 |
0.02 |
0.04 |
0.12 |
0.12 |
0.18 |
0.28 |
0.5 |
| non-linearity |
|
|
|
|
|
|
|
|
|
| quadrature
effects in ac meas. |
0 |
0 |
0 |
0 |
0 |
0 |
0 |
0 |
0 |
| |
|
|
|
|
|
|
|
|
|
|
| |
Total
A |
0.03 |
0.07 |
0.02 |
0.04 |
0.12 |
0.12 |
0.18 |
0.28 |
0.50 |
| |
n |
266 |
260 |
288 |
84 |
302 |
36 |
406 |
130 |
98 |
| Type
B |
|
|
|
|
|
|
|
|
|
|
| components
not divided by sqrt(3) |
Chemical
Impurities |
0.05 |
0.01 |
0.01 |
0.05 |
0.01 |
0.05 |
0.17 |
0.27 |
0.29 |
| Hydrostatic-head |
0.0004 |
0.0112 |
0.0032 |
0.0084 |
0.0065 |
0.0090 |
0.0092 |
0.0083 |
0.0097 |
| Propagated
TPW |
0.0018 |
0.0075 |
0.0101 |
0.0151 |
0.0182 |
0.0219 |
0.0262 |
0.0376 |
0.0538 |
| SPRT
self-heating |
0.0136 |
0.0146 |
0.0149 |
0.0155 |
0.0159 |
0.0164 |
0.0169 |
0.0184 |
0.0207 |
| Immersion |
0.0033 |
0.0071 |
0.0012 |
0.0033 |
0.0022 |
0.0030 |
0.0027 |
0.0016 |
0.0054 |
| Moisture |
0 |
0 |
0 |
0 |
0 |
0 |
0 |
0 |
0 |
| Gas
pressure |
0 |
0 |
1
E-5 |
1
E-5 |
1
E-5 |
1
E-5 |
1
E-5 |
1
E-5 |
1
E-5 |
| Insulation
degradation |
0 |
0 |
0 |
0 |
0 |
0 |
0 |
0 |
0 |
| |
|
|
|
|
|
|
|
|
|
|
| Total
B divided by sqrt(3)
|
Total
B |
0.03 |
0.01 |
0.01 |
0.03 |
0.02 |
0.03 |
0.10 |
0.16 |
0.17 |
| |
|
|
|
|
|
|
|
|
|
|
| Combined
Standard Uncertainty |
0.04 |
0.07 |
0.02 |
0.05 |
0.12 |
0.12 |
0.21 |
0.32 |
0.53 |
| |
|
|
|
|
|
|
|
|
|
|
| Expanded
Uncertainty (k=2) |
0.08 |
0.14 |
0.04 |
0.10 |
0.24 |
0.25 |
0.41 |
0.64 |
1.06 |
Top of Page
| 2/3/2000 |
|
|
TPW |
| Type
A |
|
|
mK |
| |
|
Bridge
Measurement |
|
| |
|
DR
from DT |
0 |
| repeatability
of bridge readings (n=560) |
0.003 |
| |
|
non-linearity |
|
| quadrature
effects in ac meas. |
0 |
| |
|
|
|
| |
|
Total
A |
0.003 |
| |
|
|
|
| Type
B |
|
|
|
| components
not divided by sqrt(3) |
|
Chemical
Impurities (7N5) |
0.0052 |
| |
|
Hydrostatic-head |
0.0041 |
| |
|
SPRT
self-heating |
0.0148 |
| |
|
Immersion |
0.0007 |
| |
|
Moisture |
0 |
| |
|
Gas
pressure |
0 |
| Insulation
degradation |
0 |
| |
|
|
|
| Total
B divided by sqrt(3)
|
|
Total
B |
0.01 |
| |
|
|
|
| Combined
Standard Uncertainty |
0.01 |
| |
|
|
|
| Expanded
Uncertainty (k=2) |
0.02 |
Top of Page
|
NIST
Expanded Uncertainty (k=2) for each of the ITS-90 defining fixed
points
|
|
|
|
|
|
Thermometric
fixed point
|
Temperature, K
|
U
(k=2), mK
|
|
e-H2
TP
|
13.8033
|
0.22
|
|
e-H2
VP
|
17
|
0.21
|
|
e-H2
VP
|
20.3
|
0.22
|
|
Ne
TP
|
24.5561
|
0.26
|
|
O2
TP
|
54.3584
|
0.18
|
|
AR
TP
|
83.8058
|
0.08
|
|
Hg
TP
|
234.3156
|
0.14
|
|
H2O
TP
|
273.16
|
0.02
|
|
GA
MP
|
302.9146
|
0.04
|
|
In
FP
|
429.7485
|
0.1
|
|
Sn
FP
|
505.078
|
0.24
|
|
Zn
FP
|
692.677
|
0.41
|
|
Al
FP
|
933.473
|
0.64
|
|
Ag
FP
|
1234.93
|
1.06
|
Top of Page
|
Maximum
Expanded Uncertainties (k=2) of SPRT calibrations at NIST
|
|
|
|
ITS-90
Temperature Subrange
|
U
(k=2), mK
|
|
13.8033 K
|
to
|
0.01 °C
|
0.62
|
|
54.3584
K
|
to
|
0.01 °C
|
0.29
|
|
83.8058 K
|
to
|
0.01 °C
|
0.27
|
|
234.3156 K
|
to
|
29.7646 °C
|
0.14
|
|
0
°C
|
to
|
29.7646 °C
|
0.04
|
|
0
°C
|
to
|
156.5985 °C
|
0.10
|
|
0
°C
|
to
|
231.928 °C
|
0.24
|
|
0
°C
|
to
|
419.527 °C
|
0.41
|
|
0
°C
|
to
|
660.323 °C
|
0.64
|
|
0
°C
|
to
|
961.78 °C
|
1.06
|
Top
of Page
Liquid-in-Glass
Thermometer Calibration Uncertainties
Table 6: Tolerances
and"Estimated" Uncertainties for Low-Temperature Total-Immersion
Thermometers
| Celsius
Scale Graduated Thermometers |
| |
|
|
|
|
|
Temperature
Range °C
|
Type
of Thermometer
|
Graduation
Interval in °C
|
Tolerance
in °C
|
"Estimated"
Uncertainty in °C
|
|
-35
to 0
|
Mercury
|
1.0
or 0.5
|
0.5
|
0.1
to 0.2
|
|
-35
to 0
|
Mercury
|
0.2
|
0.4
|
0.02
to 0.05
|
|
-56
to 0
|
Mercury-thallium
|
0.5
|
0.5
|
0.1
to 0.2
|
|
-56
to 0
|
Mercury-thallium
|
0.2
|
0.4
|
0.02
to 0.05
|
|
-200
to 0
|
Organic
Liquid
|
1
|
2
|
0.2
to 0.5
|
|
|
|
|
|
|
|
Fahrenheit
Scale Graduated Thermometers
|
|
|
|
|
|
|
|
Temperature
Range °F
|
Type
of Thermometer
|
Graduation
Interval in °F
|
Tolerance
in °F
|
"Estimated"
Uncertainty in °F
|
|
-35
to 32
|
Mercury
|
1.0
or 0.5
|
1
|
0.1
to 0.2
|
|
-35
to 32
|
Mercury
|
0.2
|
0.5
|
0.04
|
|
-69
to 32
|
Mercury-thallium
|
1.0
or 0.5
|
1
|
0.1
to 0.2
|
|
-69
to 32
|
Mercury-thallium
|
0.2
|
0.5
|
0.04
|
|
-328
to 32
|
Organic
Liquid
|
2.0
or 1.0
|
3
|
0.3
to 0.5
|
Top of Page
Table 7: Tolerances and
"Estimated" Uncertainties for Low-Temperature Partial-Immersion
Thermometers, where "Estimated" Uncertainties are calculated
using values from BS Circular No. 8 (1921).
| Celsius
Scale Graduated Thermometers |
| |
|
|
|
|
|
Temperature
Range °C
|
Type
of Thermometer
|
Graduation
Interval in °C
|
Tolerance
in °C
|
"Estimated"
Uncertainty in °C
|
|
-35
to 0
|
Mercury
|
1.0
or 0.5
|
0.5
|
0.2
to 0.3
|
|
-56
to 0
|
Mercury-thallium
|
1.0
or 0.5
|
0.5
|
0.2
to 0.3
|
|
-90
to 0
|
Organic
Liquid
|
1
|
3
|
0.4
to 1.0
|
| |
|
|
|
|
| Fahrenheit
Scale Graduated Thermometers |
| |
|
|
|
|
|
Temperature
Range °F
|
Type
of Thermometer
|
Graduation
Interval in °F
|
Tolerance
in °F
|
"Estimated"
Uncertainty in °F
|
|
-35
to 32
|
Mercury
|
1.0
or 0.5
|
1
|
0.3
to 0.5
|
|
-69
to 32
|
Mercury-thallium
|
1.0
or 0.5
|
1
|
0.3
to 0.5
|
|
-130
to 32
|
Organic
Liquid
|
2.0
or 1.0
|
5
|
0.8
to 2.0
|
Top of Page
Table 8: Tolerances and"Estimated"
Uncertainties for Celsius Total-Immersion Mercury Thermometers
|
Temperature
range in °C
|
Graduation
interval
in °C
|
Tolerance
in °C
|
"Estimated"
Uncertainty
in °C
|
|
|
|
|
|
|
Thermometers
Graduated below 150 °C
|
|
0
up to 150
|
1.0
or 0.5
|
0.5
|
0.1
to 0.2
|
|
0
up to 150
|
0.2
|
0.4
|
0.02
|
|
0
up to 150
|
0.1
|
0.3
|
0.02
|
|
|
|
|
|
|
Thermometers
graduated below 300 °C
|
|
0
up to 100
|
1.0
or 0.5
|
0.5
|
0.05
|
|
Above
100 up to 300
|
1.0
or 0.5
|
1
|
0.05
|
|
0
up to 100
|
0.2
|
0.4
|
0.02
|
|
Above
100 up to 200
|
0.2
|
0.5
|
0.06
|
|
|
|
|
|
|
Thermometers
graduated above 300 °C
|
|
0
up to 300
|
2
|
2
|
0.2
to 0.5
|
|
Above
300 up to 500
|
2
|
4
|
0.05
to 1.0
|
|
0
up to 300
|
1.0
or 0.5
|
2
|
0.16
|
|
Above
300 up to 500
|
1.0
or 0.5
|
4
|
0.16
|
Top of Page
Table 9: Tolerances and"Estimated"
Uncertainties for Fahrenheit Total-Immersion Mercury Thermometers
|
Temperature
range in °F
|
Graduation
interval
in °F
|
Tolerance
in °F
|
"Estimated"
Uncertainty
in °F
|
|
|
|
|
|
|
Thermometers
Graduated below 300 °F
|
|
32
up to 300
|
1.0
or 0.5
|
0.5
|
0.1
to 0.2
|
|
32
up to 300
|
0.2
|
0.4
|
0.02
|
|
32
up to 212
|
0.1
|
0.3
|
0.02
|
|
|
|
|
|
|
Thermometers
graduated below 600 °F
|
|
32
up to 212
|
2.0
or 1.0
|
1
|
0.2
to 0.5
|
|
Above
212 up to 600
|
2.0
or 1.0
|
2
|
0.5
|
|
|
|
|
|
|
Thermometers
graduated above 600 °F
|
|
32
up to 600
|
5
|
4
|
0.5
to 1.0
|
|
Above
600 up to 950
|
5
|
7
|
1.0
to 2.0
|
|
32
up to 600
|
2.0
or 1.0
|
3
|
0.2
to 1.0
|
|
Above
600 up to 950
|
2.0
or 1.0
|
6
|
0.5
to 1.0
|
Top of Page
Table 10: Tolerances and
"Estimated" Uncertainties for Celsius Partial-Immersion Mercury
Thermometers
|
Temperature
range
in °C
|
Graduation
interval
in °C
|
Tolerance
in °C
|
"Estimated"
Uncertainty
in °C
|
|
|
|
|
|
|
Thermometers
Graduated below 150 °C
|
|
0
up to 100
|
1.0
or 0.5
|
1
|
0.1
to 0.3
|
|
0
up to 150
|
1.0
or 0.5
|
1
|
0.1
to 0.5
|
|
|
|
|
|
|
Thermometers
graduated below 300 °C
|
|
0
up to 100
|
1
|
1
|
0.1
to 0.3
|
|
Above
100 up to 300
|
1
|
1.5
|
0.5
to 1.0
|
|
|
|
|
|
|
Thermometers
graduated above 300 °C
|
|
0
up to 300
|
2.0
or 1.0
|
2.5
|
0.5
to 1.0
|
|
Above
300 up to 500
|
2.0
or 1.0
|
5
|
1.0
to 2.0
|
|